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Category:Photographic softwareInorganic/organic magnetic composite microcapsules: synthesis and their potential applications in solid-phase extraction coupled with HPLC-UV analysis.
Inorganic/organic magnetic (IO) composite microcapsules with high specific surface area (SSA) were synthesized by a novel one-step synthesis without using any surfactants and organic solvents. The characterization results showed that IO microcapsules were spherical in shape and encapsulated both the inorganic and organic fillers into the polymeric matrix. The average diameter of IO microcapsules obtained was ∼188 μm, and the average yield of encapsulation was 81.8 ± 0.9%. The Brunauer-Emmett-Teller (BET) surface area of IO microcapsules was calculated to be ∼2426 m(2) g(-1). The IO microcapsules demonstrated excellent magnetic responsiveness at a low concentration (4.5 × 10(-6) M), and the maximum magnetization value is 45 mT. In addition, the number of Fe(3+) ions per unit mass of IO microcapsules was estimated to be 3.46 × 10(-6) M. The IO microcapsules could be utilized as a solid-phase extraction (SPE) sorbent for pre-concentration of low-concentration metal ions (e.g., Cd(2+) and Pb(2+)) prior to their determination by using high-performance liquid chromatography with UV detector (HPLC-UV). Under optimum conditions, good linearity was obtained for the spiked analysis (0.5-5 μM), and the relative standard deviation (RSD) of the method for five successive analysis of 0.5 μM Cd(2+) was 1.55%. The LOQ of Cd(2+) was as low as 0.13 μM. The developed method was successfully applied to the determination of trace amounts of Cd(2+) in some real samples (e.g., environmental water samples).Diversity
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