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The method presented in this paper is designed to collect and purify radiolabelled phosphate in the femur of rats. Bones are immersed in 2 ml of saline containing 1 mg of buffer phosphate. After homogenization, the samples are centrifuged at low speed and the supernatants are obtained. The phosphate is extracted from the sample using 1 ml of 0.3 M NaOH, and separated from organic substances, which are also removed, using Dowex 50WX4, in acidic conditions. The purified radiolabelled phosphate is eluted from the column using 2 ml of 1 M HCl. The combination of these procedures resulted in the collection of 21, 12.2 and 3.3% of the injected dose per bone for 45 min, 5 h and 24 h, respectively.[Effects of the structure of bulks based on new metal-organic framework MIL-53 on the adsorption of low-molecular organic compounds].
The effects of the structure of bulks based on new metal-organic frameworks MIL-53 on the adsorption of low-molecular organic compounds was investigated. Comparing with the bulk-MIL-53-based bulks synthesized by traditional solid-liquid mixing approach, bulks based on MOFs with three different structures, cubocta